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Optimization of the methods for small peptide solution structure determination by NMR spectroscopy

โœ Scribed by A. N. Istrate; A. B. Mantsyzov; S. A. Kozin; V. I. Polshakov


Book ID
110174874
Publisher
SP MAIK Nauka/Interperiodica
Year
2010
Tongue
English
Weight
516 KB
Volume
44
Category
Article
ISSN
0026-8933

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The structure of the vasoactive intestinal peptide 1-28 in 40% 2,2,2-trifluoroethanol was investigated by two-dimensional 'H-nmr spectroscopy. All 'H resonances, except the y, 6, and c protons of the lysine residues, could be sequentially assigned. Numerous intraresidual as well as short-range inter