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Optimization of texturing process by hot pressing of Bi-Pb-Sr-Ca-Cu-O (2223) ceramics

✍ Scribed by J.G. Noudem; J. Beille; D. Bourgault; A. Sulpice; R. Tournier


Publisher
Elsevier Science
Year
1994
Tongue
English
Weight
748 KB
Volume
230
Category
Article
ISSN
0921-4534

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✦ Synopsis


We have optimized a texturing process of Bi-Pb-Sr-Ca-C'u-O (2223) superconducting ceramics by hot pressing. The Hoechst precursor powder has been first pressurized at 1 GPa and then heated under uniaxial stress up to 35 MPa, just below the melting temperature between 850°C and 857°C. We have obtained large textured samples having critical transport current densities Jc as large as 2500 A/cm 2. In this work, we have optimized the stress value as well as the temperature treatment on the basis of characterizations such as magnetization and electrical-transport measurements.


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Preparation of superconducting BiPbSr
✍ E. Yanmaz; J.S. Abell; I.R. Harris 📂 Article 📅 1991 🏛 Elsevier Science 🌐 English ⚖ 395 KB

Bi-pb-Sr-Ca-Cu-O bulk samples with nominal composition of Bil.6Pb0.4Sr2Ca3Cu4Oy (2234) were prepared by a melt casung method. The melting process was carried out on two different powders; one consisting of the precursor materials, and one in which the precursor had been calci,r,d.Th~-~ffects of the