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Optimization of 1 H and 13 C NMR Methods for Structural Characterization of Acetone and Pyridine Soluble/Insoluble Fractions of a Coal Tar Pitch

✍ Scribed by Morgan, Trevor J.; George, Anthe; Davis, David B.; Herod, Alan A.; Kandiyoti, Rafael

Book ID
126407616
Publisher
American Chemical Society
Year
2008
Tongue
English
Weight
176 KB
Volume
22
Category
Article
ISSN
0887-0624

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1H-1,3-Diazepines, 5H-1,3-diazepines, 1,3-diazepinones, and 2,4-diazabicyclo[3.2.0]heptenesPreliminary reports on parts of this work have been published in ref 1. This paper is Diazepines, Part 3. For Part 2, see ref 2.,Electronic supplementary information (ESI) available: NMR spectra of 4a, 4c, 19v ? 20, 19a ? 25a, and 19g ? 25g (Fig. S1?S6), Arrhenius and Eyring plots for H-exchange in 4b,c (Fig. S7), views of the X-ray crystal structures of compounds 26 and 22bB (Fig. S8?S9), bond lengths and angles for compounds 4k, 22bB and 26, preparative procedures and characterization data for all compounds not described in the Experimental section, and computational data (Cartesian coordinates, absolute energies, IR, 1H and 13C NMR) for 20a?c, 21a?b, 22aA?F and 22aB dimer. See http://www.rsc.org/suppdata/ob/b3/b317099c/
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