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Optimization and Scale-Up of a Suzuki−Miyaura Coupling Reaction: Development of an Efficient Palladium Removal Technique

✍ Scribed by Bullock, Kae M.; Mitchell, Mark B.; Toczko, Jennifer F.

Book ID: 120363019
Publisher: American Chemical Society
Year: 2008
Tongue: English
Weight: 625 KB
Volume: 12
Category: Article
ISSN: 1083-6160
DOI: 10.1021/op800064y

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## Abstract Four palladium chelate complexes with S‐ or Se‐containing substituted salicylaldehyde Schiff‐base derivatives have been synthesized. Spectroscopic and crystallographic data indicate that, in the complexes, the deprotonated salicylaldehyde ligand is bound to the metal in an O,N,S (or Se)