A convenient one-pot synthesis of [1]benzothieno [3,2-b]benzothiophene from readily available o-dihalostilbenes using combined reagents of sodium sulfide nonahydrate (Na 2 SΓ9H 2 O) or sodium hydrosulfide hydrate (NaSHΓnH 2 O) and sulfur is described along with plausible reaction paths in this intri
β¦ LIBER β¦
One-step synthesis of [1]benzothieno[3,2-b][1]benzothiophene from o-chlorobenzaldehyde
β Scribed by Masahiko Saito; Itaru Osaka; Eigo Miyazaki; Kazuo Takimiya; Hirokazu Kuwabara; Masaaki Ikeda
- Publisher
- Elsevier Science
- Year
- 2011
- Tongue
- French
- Weight
- 492 KB
- Volume
- 52
- Category
- Article
- ISSN
- 0040-4039
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β¦ Synopsis
Simple one-step synthesis of [1]benzothieno [3,2-b][1]benzothiophene (BTBT) from commercially available o-chlorobenzaldehyde is reported. The procedure is also applicable to the synthesis of dinaphtho[2,3-b:2 0 ,3 0 -f]thieno[3,2-b]thiophene (DNTT).
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## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 200 leading journals. To access a ChemInform Abstract, please click on HTML or PDF.
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