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One step conversion of anilines to aryl halides using sodium nitrite and halotrimethylsilane

✍ Scribed by Jong Gun Lee; Hee Tae Cha

Book ID: 104216226
Publisher: Elsevier Science
Year: 1992
Tongue: French
Weight: 165 KB
Volume: 33
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(00)79842-x

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✦ Synopsis

Anilines were easily diazotized and efficiently converted to aryl halides in un one-pot reaction using sodium nitrite and halotrimethylsilane in carbon tetrachloride. Haiotrimethylsilanes are used for both generating nitrosonium donor from sodium nitrite, and the halogen substitution of diazonium group.

Continuous

search of useful functional group transformation reactions using halotrimethylsilane-inorganic oxide or salt pairs has been fruitful'.

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