2-Dimethoxyphosphoryl-l,3-dithiane was obtained by the reaction of 2-ddoro-1,3&thia~~e with trimethyl phosphite. Studies at 200,360 and 400 MHz using 'H, 13C and " P nuclei and lDand 2D NMR techniques are described. Long-range coupling constants were extracted by iterative treatment of [ A B ] , C D
One-dimensional13C NMR and HPLC-1H NMR techniques for observing carbon-13 and deuterium labelling in biosynthetic studies
✍ Scribed by Bernd Schneider; Jonathan Gershenzon; Gerson Graser; Dirk Hölscher; Bettina Schmitt
- Book ID
- 111604139
- Publisher
- Springer
- Year
- 2003
- Tongue
- English
- Weight
- 215 KB
- Volume
- 2
- Category
- Article
- ISSN
- 1568-7767
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