One and Two Dimensional NMR Spectroscopy

✍ Scribed by Atta-ur- Rahman (Auth.)

• Publisher: Elsevier Science Ltd
• Year: 1989
• Tongue: English
• Leaves: 576
• Category: Library

✦ Synopsis

The field of nuclear magnetic resonance spectroscopy has undergone explosive development during the last decade with the advent of new one- and two-dimensional techniques. The author has had extensive experience in the use of these techniques for the structure elucidation of complex natural products, and in this book he gives a comprehensive, up-to-date and very readable account of these developments. The book's scope is very wide. It starts from fundamental principles of modern NMR spectroscopy, describing the instrumentation and its optimum use, and extends to the latest developments such as inverse measurements. Emphasis is on problem-solving so as to be useful to a large number of organic chemists, biochemists and medicinal chemists. The problems and worked solutions at the end of the chapters will help students to gain proficiency in the application of these new techniques. Those who are learning how to operate modern NMR spectrometers will find particularly useful the description of such basic aspects as shimming, probe tuning, and methods for improvement of resolution and sensitivity

✦ Table of Contents

Content:
Front Matter, Page III
Copyright, Page IV
PREFACE, Pages V-VI
FOREWORD, Pages VII-VIII
Chapter 1 - Basic Principles of Modern NMR Spectroscopy, Pages 1-75
Chapter 2 - Spin-Echo and Polarisation Transfer, Pages 77-140
Chapter 3 - Carbon-Carbon Connectivity-1D-INADEQUATE Spectra, Pages 141-165
Chapter 4 - The Nuclear Overhauser Effect, Pages 167-201
Chapter 5 - Two-Dimensional NMR Spectroscopy — Basic Principles, Pages 203-215
Chapter 6 - Heteronuclear 2D J-Resolved Spectroscopy, Pages 217-243
Chapter 7 - Homonuclear 2D J-Resolved Spectroscopy, Pages 245-267
Chapter 8 - Homonuclear 2D Shift Correlated Spectroscopy, Pages 269-358
Chapter 9 - Chemical Shift Correlation Through Cross-Relaxation and Exchange, Pages 359-390
Chapter 10 - Heteronuclear 2D Shift Correlation Spectroscopy, Pages 391-434
Chapter 11 - Cross-Polarisation in the Rotating Frame, Pages 435-446
Chapter 12 - 2D Multiple-Quantum Spectroscopy, Pages 447-491
Chapter 13 - Tackling the Structure, Pages 493-510
Chapter 14 - Product Operators Approach to 2D-NMR Spectroscopy, Pages 511-526
Appendix 1 - SOME TERMS, SYMBOLS AND ACRONYMS USED IN NMR SPECTROSCOPY, Pages 527-536
Appendix 2 - SUMMARY OF IMPORTANT 2D NMR TECHNIQUES, Pages 537-551
INDEX, Pages 553-578