On the crystal structures of methylamine
β Scribed by Atoji, M. ;Lipscomb, W. N.
- Book ID
- 118689899
- Publisher
- International Union of Crystallography
- Year
- 1953
- Tongue
- English
- Weight
- 505 KB
- Volume
- 6
- Category
- Article
- ISSN
- 0365-110X
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A straightforward preparation has been found for bis(dichlorosilyl)methylamine, (SiHCl 2 ) 2 NMe (1), involving reaction between H 2 NMe and an excess of SiHCl 3 , dissolved either in pentane or THF at 253 K. 1 and a side-product, 1,3,5-trichloro-2,4,6-trimethylcyclotrisilazane, (Β±SiHClΒ±NMeΒ±) 3 (2),