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On the calculation of gibbs energy corresponding to enantioselective interactions at a direct HRGC separation of enantiomers

✍ Scribed by Ján Krupcík; Ivan Spánik; Peter Oswald; Pavol Májek; Ivan Skacáni; Pat Sandra


Publisher
John Wiley and Sons
Year
2000
Tongue
English
Weight
244 KB
Volume
12
Category
Article
ISSN
0899-0042

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✦ Synopsis


A novel procedure is proposed for the calculation of Gibbs energy corresponding to enantiospecific interactions of 2-(2,4-dinitrophenoxy)-, 2-phenoxy-, and 2-halogen-n-pentane enantiomers with a ␤-cyclodextrin (ChirasilDex) stationary phase under gas chromatographic conditions. This energy is calculated from retention data as a difference between the Gibbs energy of an enantiomer and its corresponding achiral congener. The procedure for the determination of 2-(2,4-dinitrophenoxy)-, 2-phenoxyand 2-halogen-n-pentane achiral congener retention data is discussed in detail.