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On-line coupling of high temperature GPC and 1H NMR for the analysis of polymers

✍ Scribed by Wolf Hiller; Harald Pasch; Tibor Macko; Martin Hofmann; Jürgen Ganz; Manfred Spraul; Ulrich Braumann; Roman Streck; Jeff Mason; Freddy Van Damme


Book ID
108184798
Publisher
Elsevier Science
Year
2006
Tongue
English
Weight
825 KB
Volume
183
Category
Article
ISSN
1090-7807

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High-temperature and high-pressure 1H NM
✍ S. Shimokawa; E. Yamada; T. Yokono; S. Iyama; Y. Sanada 📂 Article 📅 1984 🏛 Elsevier Science 🌐 English ⚖ 321 KB

An autoclave-type 'H NMR probe has been developed to monitor the carbonization process of such carbonaceous materials as coal and pitch under high pressures up to 10 MPa. In the early stages of the carbonization of pitch, the change in hydrogen aromaticity, fHe, was found to be dependent on the appl