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Observation of an incommensurate phase in the stable phase sequence of deuterated thiophene by powder neutron diffraction

✍ Scribed by Frédéric Dunstetter; Daniel André; Anne Gonthier-Vassal; Henri Szwarc; Nicole Ratovelomanana; Marie-France Lautie

Book ID
107942851
Publisher
Elsevier Science
Year
1993
Tongue
English
Weight
652 KB
Volume
175
Category
Article
ISSN
0301-0104

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Localisation of excess oxygen in the hig
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✍ G. Miehe; T. Vogt; H. Fuess; M. Wilhelm 📂 Article 📅 1990 🏛 Elsevier Science 🌐 English ⚖ 294 KB

Neutron and X-ray powder diffractograms of the title compound were refined by the Rietveld method. Within the bismuth layer an additional oxygen site with population parameter 0.12 was found which is interpreted as the excess oxygen. From the comparison of population parameters from neutron and X-ra