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Observation and interpretation of HH coupling in 1H187Os satellite NMR spectra

✍ Scribed by Jennifer S. Holmgren; John R. Shapley; Patricia A. Belmonte


Publisher
Elsevier Science
Year
1985
Tongue
English
Weight
264 KB
Volume
284
Category
Article
ISSN
0022-328X

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187Os subspectra in 1H and 31P{1H} spect
✍ Marc J. Stchedroff; Silvio Aime; Roberto Gobetto; Luca Salassa; Ebbe Nordlander 📂 Article 📅 2002 🏛 John Wiley and Sons 🌐 English ⚖ 151 KB

## Abstract A survey of the use of ^187^Os satellite subspectra in ^1^H and ^31^P{^1^H} spectra of triosmium carbonyl clusters is reported. By varying evolution delays in HMQC spectra of [Os~3~(µ‐H)~2~(CO)~10~] we have selectively extracted the values for ^1^__J__(Os,H) and ^2^__J__(Os,H), respecti