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O-allyl ether as a new protective group for oximes and its palladium-catalyzed deprotection

✍ Scribed by Toshiro Yamada; Kuniaki Goto; Yasuhiro Mitsuda; Jiro Tsuji


Publisher
Elsevier Science
Year
1987
Tongue
French
Weight
242 KB
Volume
28
Category
Article
ISSN
0040-4039

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✦ Synopsis


Oximes are protected by O-ally1 ether formation, and their palladium-catalyzed deallylation using triethylammonium formate as a reductant proceeds smoothly in boiling ethanol under mild conditions offering a good protective method for oximes.

Oxime formation offers a good protection for carbonyl groups.') However,