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Nucleosides LXXVII. Rotational isomerism of certain 3-β-D-glucopyranosyl-6-methyluracils

✍ Scribed by K.A. Watanabe; S.S. Saluja; B.A. Otter; J.J. Fox

Book ID: 104245275
Publisher: Elsevier Science
Year: 1972
Tongue: French
Weight: 212 KB
Volume: 13
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(01)94194-2

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✦ Synopsis

acetyl-S-i-glucopyranosyl bromide or with tri-{-benzoyl-i-ribofuranosyl chloride by the nitromethane-Hg(CN)2 method 3 afforded the 3-glycosylated pyrimidines (1 and 2 respectively). On the basis of two pairs of doublets observed by them in the nmr spectrum of the de-acylated glucosyl derivative (3), they concluded that compounds 1 and 3 were anomeric mixtures. Further, --

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