✦ LIBER ✦

Nuclear Magnetic Resonance Studies of Tertiary Phosphines Adducts with Titanium Tetrachloride, using 1H and 31P

✍ Scribed by F. Calderazzo; S. A. Losi; B. P. Susz

Publisher: John Wiley and Sons
Year: 1971
Tongue: German
Weight: 943 KB
Volume: 54
Category: Article
ISSN: 0018-019X
DOI: 10.1002/hlca.19710540425

No coin nor oath required. For personal study only.

✦ Synopsis

Reflexionszusatz. wurden die Festkiirfierspektren crhalten. Die Substanzen wurden dazu rnit Bariumsulfat verdiinnt unrl gegen Hariunisulfat als Weiss-Standard vermesscn. -InfravolspPktren wurtlen mit denil registrierenden Infrarotspektrophotometcr Beckmuiz IR-12 aufgenommen. Fiir die Losungsspektren in Methylenbromid wurden Polyathylenkuvctten von 0 , l cm Schichtdickc vcrmendet. I:ur die Festkorperspektren wurden die I<omplexe in Kujol zcrrieben und zwischen I-'olyathylenplatl:en prapariert.

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