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Nuclear Magnetic Resonance Spectrum of a Diastereomer of Quercitol (Deoxyinositol). Synthesis of allo-Quercitol and its 6-Chloro, 6-Bromo and 6-Iodo Derivatives 1,2

✍ Scribed by Shoolery, J. N.; Johnson, L. F.; Furuta, Stanley; McCasland, G. E.

Book ID: 126118047
Publisher: American Chemical Society
Year: 1961
Tongue: English
Weight: 727 KB
Volume: 83
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja01481a035

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## Abstract The influence of substituents in a new series of 2__H__‐thiopyrans, 2__H__‐thiopyran‐2‐ones (thiones) and their thiazine analogues is examined by means of carbon (^13^C) and nitrogen (^15^N) NMR. A linear relationship is shown to exist between the chemical shifts (δ~13C~ or δ~15N~) of t