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Nuclear magnetic resonance of 27Al in single crystals of NaMgAl(C2O4)3·xH2O

✍ Scribed by W.T. Zbieranowski

Publisher
Elsevier Science
Year
1975
Tongue
English
Weight
346 KB
Volume
36
Category
Article
ISSN
0009-2614

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✦ Synopsis

Nudear magnetic resonance of " Al nuclei wns used to determine the quadrupole splitting constants vQ of the A? ion in the oxalate complexes of h'a.hlgAl(C:!0$!3-8H20 and NahigAl(C204)3-9H20.

The eightfold-hydrated crystal was obhined by annealing a nkefold-hydrated crystal. The resonance spectrum of the ninefold-hydrated crystal is split and the asymmetry prrrameter r) amounts to 0.076.

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hfagnctic amsotropres of a tr~gonal crystal of NahlgCr(C204)3-9H20 measured between 300 and 77 I: arc appro~lmatcly inversely proportional IO the square of the absolute temperature; moreover KII > K, although gl > g,, from EPR measuremcnts The sign of D, the zero-field sphttmg. wtuch was not dctcrmm