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Novel three-dimensional1H−13C−31P triple resonance experiments for sequential backbone correlations in nucleic acids

✍ Scribed by Gabriele Varani; Fareed Aboul-ela; Frederic Allain; Charles C. Gubser


Book ID
104666808
Publisher
Springer Netherlands
Year
1995
Tongue
English
Weight
511 KB
Volume
5
Category
Article
ISSN
0925-2738

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A 3D triple resonance experiment has been designed to provide intraresidual and sequential correlations between amide nitrogens and c~-carbons in uniformly 13C/15N-labeled proteins. In-phase 13C~ magnetization is transferred to the aliphatic side-chain protons via the side-chain carbons using a CC-T