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Novel synthetic approaches to the palmarumycin skeleton

✍ Scribed by Ian G.C Coutts; Robert W Allcock; Hans W Scheeren

Publisher: Elsevier Science
Year: 2000
Tongue: French
Weight: 79 KB
Volume: 41
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(00)01625-7

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✦ Synopsis

Oxidation of readily available aminonaphthols 7a and 7b with activated manganese dioxide gives palmarumycin analogues 8a and 8b in good yield. The related benzoquinone monoacetals 10a-c undergo cycloaddition with 3-methoxy-2-pyrone at high pressure to give adducts 12a-c, also possessing the palmarumycin framework.

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