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Novel Biocatalysts by Chemical Modification of Known Enzymes: Cross-Linked Microcrystals of the Semisynthetic Peroxidase Seleno-Subtilisin

✍ Scribed by Dietmar Häring; Peter Schreier


Publisher
John Wiley and Sons
Year
1998
Tongue
English
Weight
96 KB
Volume
37
Category
Article
ISSN
0044-8249

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✦ Synopsis


The linkage of lysine residues on the surfaces of subtilisin crystals (NH -Enz; see Scheme) with glutardialdehyde affords an immobilized biocatalyst of high stability and purity. The replacement of the serine OH group in the active site (Enz-OH) by SeO H leads to new activity as a peroxidase. Thus for the first time, chemical enzyme engineering has resulted in a biocatalyst with a modified peptide framework as well as a new catalytically active site. This methodology combines reasonable substrate selectivity of a semisynthetic enzyme with the exceptional stability of cross-linked enzyme crystals.