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Notes - Reaction of Ethyl Acrylate with Methyl n-hexyl Ketone

✍ Scribed by Miller, John; de Benneville, Peter

Book ID
127088776
Publisher
American Chemical Society
Year
1957
Tongue
English
Weight
283 KB
Volume
22
Category
Article
ISSN
0022-3263

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Baylis–Hillman reactions of N-arylidened
Baylis–Hillman reactions of N-arylidenediphenylphosphinamides with methyl vinyl ketone, methyl acrylate, and acrylonitrile
✍ Min Shi; Gui-Ling Zhao 📂 Article 📅 2002 🏛 Elsevier Science 🌐 French ⚖ 70 KB

We have found that in the Baylis-Hillman reactions of N-arylidenediphenylphosphinamides 1 with methyl vinyl ketone (MVK), methyl acrylate or acrylonitrile, the Lewis base and solvent can significantly affect the reaction rate. Using PPh 3 as Lewis base in the reaction of 1 with MVK in DMF, THF or Me