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Non-isothermal, in situ XRD analysis of dolomite decomposition

✍ Scribed by Philip Engler; Mark W. Santana; Martin L. Mittleman; David Balazs


Publisher
Elsevier Science
Year
1989
Tongue
English
Weight
524 KB
Volume
140
Category
Article
ISSN
0040-6031

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Non-isothermal, in situ XRD analysis of
✍ Philip Engler; Mark W. Santana; Martin L. Mittleman; David Balazs πŸ“‚ Article πŸ“… 1989 πŸ› Elsevier Science 🌐 English βš– 524 KB

In situ X-ray diffraction (XRD) was used to elucidate the thermal decomposition of dolomite. As opposed to previous efforts that required samples be heated to a specific temperature and held for the duration of an X-ray scan, data was collected at 4O C intervals while continuously heating the sampl

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## Abstract The decomposition of ammonium heptamolybdate (AHM, (NH~4~)~6~Mo~7~O~24~Γ—4H~2~O) was studied in situ by X‐ray diffraction and X‐ray absorption spectroscopy, as well as by thermal analysis (TG/DTA). Decomposition conditions such as reactant atmospheres, (20% oxygen, 5% propene, 5% hydroge