The title compound, C 24 H 18 N 2 O 4 ÁC 2 H 6 OS, adopts an anti C O conformation. The two amide groups are twisted away from the attached central ring by 48.48 (5) and 46.49 (5) . In the crystal structure, the molecules are connected by O-HÁ Á ÁO and N-HÁ Á ÁO hydrogen bonds, forming a twodimensio
N,N′-Di-2-pyridylbenzene-1,3-dicarboxamide dimethyl sulfoxide solvate
✍ Scribed by Qin, Da-Bin ;Jin, Lin-Hai ;zhang, Huan-Xia ;Gu, Shao-Jin
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 145 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
In the title compound, C 23 H 17 N 5 O 2 S 2 ÁC 3 H 7 NO, hydrogen bonds involving the amide groups and the pyridine N atoms force the two carboxamide groups and the central pyridine ring into the same plane. The solvent molecule is stabilized in the cavity formed by the two arms of the molecule by
The crystal structure of the title compound, C 29 H 29 N 3 O 3 , is stabilized by weak N-HÁ Á ÁO hydrogen bonds. In the title compound, the dihedral angles between the pyrrolidine ring and the phenyl rings are 75.2 (2), 76.6 (2) and 77.2 (2) , respectively.
Single-crystal X-ray study T = 293 K Mean (C-C) = 0.006 A Disorder in solvent or counterion R factor = 0.041 wR factor = 0.092 Data-to-parameter ratio = 12.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.