NMR Spectroscopy and Conformational Features
β Scribed by R. J. Ferrier; R. Blattner; R. A. Field; R. H. Furneaux; J. M. Gardiner; J. O. Hoberg; K. P. R. Kartha; D. M. G. Tilbrook; P. C. Tyler; R. H. Wightman
- Publisher
- John Wiley and Sons
- Year
- 2010
- Weight
- 24 KB
- Volume
- 33
- Category
- Article
- ISSN
- 0931-7597
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β¦ Synopsis
Abstract
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Complete 1H and 13C spectrum of a polysaccharide isolated from Escherichia coli, which is the major component of the enterobacterial common antigen, has been analyzed through two-dimensional nuclear magnetic resonance spectroscopy. In addition, distance constraints from NOESY and ROESY experiments h
3 a ) and (3c) or (Sf) formed as minor products on reaction ( I ) with methyl acryiate or methyl propiolate were synthesized isomer-free from the diester (1') and characterized. The data for the compounds prepared are summarized in Table .