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NMR spectra and structure of 2-(2′-chloroethoxy)-2-oxa-3-methyl-1,4,2-dioxaphosphane

✍ Scribed by M. V. Sigalov; V. A. Pestunovich; V. I. Glukhikh; M. Ya. Khil'ko; V. M. Nikitin; M. F. Larin; B. A. Trofimov

Book ID
112480578
Publisher
Springer
Year
1975
Tongue
English
Weight
240 KB
Volume
24
Category
Article
ISSN
1573-9171

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✍ Jorma Mattinen; Kalevi Pihlaja 📂 Article 📅 1987 🏛 John Wiley and Sons 🌐 English ⚖ 209 KB

I7O NMR chemical shifts of 2-oxo-1,3,2-dioxathiane and 13 of its methyl-substituted derivatives are reported. The chemical shifts depend strongly on temperature and to a much smaller extent on concentration. As a whole, however, they strongly support the predominance of chair conformations in these