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NMR of 31P in (VO)2P2O7 as an internal temperature standard in high-temperature NMR

✍ Scribed by Hongjun Pan; B.C Gerstein

Book ID
107798546
Publisher
Elsevier Science
Year
1991
Weight
107 KB
Volume
92
Category
Article
ISSN
0022-2364

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Squaric acid as an internal standard for
Squaric acid as an internal standard for temperature measurements in 13C MAS NMR
✍ A.N. Klymachyov; N.S. Dalal πŸ“‚ Article πŸ“… 1996 πŸ› Elsevier Science 🌐 English βš– 670 KB

Squaric acid (3,4-dihydroxy-3-cyclobutene-1,2-dione) is suggested as an internal standard for temperature measurements in 13C MAS NMR studies in the temperature range from 373 K to 520 K. Compared to previously utilized standards, squaric acid has several important advantages, such as fast kinetics