NMR J cross-polarization in liquids: A refocusing method
โ Scribed by G.C Chingas; A.N Garroway; R.D Bertrand; W.B Moniz
- Publisher
- Elsevier Science
- Year
- 1979
- Weight
- 366 KB
- Volume
- 35
- Category
- Article
- ISSN
- 0022-2364
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The inverse cubic dependency of the acceleration of a rotor on its diameter allows for mechanical dynamics comparable to spin dynamics in coupled spin systems. Rotor acceleration up to 300 kHz/s was measured. This feature can be used to simplify existing experiments and explore entirely new ones in
It is generally observed that the performance of double-resonance multiple-pulse-based \(J\) cross polarization (DCP) is superior to that of pulsed-free-precession (INEPT)-based sequences for net transfer of coherence between scalar coupled spins. Here, effects of relaxation and radiofrequency field