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NMR detection of hydration water in the intermolecular interface of a protein-DNA complex

✍ Scribed by Qian, Yan Qiu; Otting, Gottfried; Wuethrich, Kurt

Book ID
127159105
Publisher
American Chemical Society
Year
1993
Tongue
English
Weight
293 KB
Volume
115
Category
Article
ISSN
0002-7863

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High-resolution \*H-nmr is employed to monitor the D20 in hydrated solids of Li-DNA prepared from solution by three different methods: lyophilization, slow evaporation of the water, and wet spinning in alcohol. From the spectral shapes and spin-spin relaxation measurements, the DNA in the lyophilize