NMR (1H, 13C, 29Si) study of some allylhalogenosilanes
โ Scribed by L. Delmulle; G.P. Van Der Kelen
- Publisher
- Elsevier Science
- Year
- 1981
- Tongue
- English
- Weight
- 282 KB
- Volume
- 70
- Category
- Article
- ISSN
- 0022-2860
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Chemical shift and scalar coupling constant data have been obtained for the 'H, -C and "Si nuclei in dyl, methallyl, cis-and trans-croty1, cis-2-methyI-2-butenyl and 3-methyl-2-butenyl derivatives of trimethylsilane.
I3C and 'H NMR spectral data for a homologous series of tertiary arsines (R,As, where R = Me, Et, n-Pr and Ph), aminoarsines and arsonium and aminoarsonium salts are reported and discussed. In nearly all cases, quaternization of the tertiary arsine to its corresponding arsonium or aminoarsonium salt
H and lSC NMR chemical shifts are reported and assigned for 1,4,9,10-and 2,3,9,1 O-anthracenetetrone. In addition, NMR data are given for 2,3-dihydroxy-9, 1 O-anthraquinone, 2.3-dimethoxy-9.10anthraquinone and 1 -hydroxy-2-acetoxy-9,l O-anthraquinone, encountered during the preparation of the anthra