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Nitrogen-coordinated complexes. Preparations and reactions of hydrido-phosphine complexes of ruthenium and rhodium

✍ Scribed by Ito, Takashi.; Kitazume, Shoji.; Yamamoto, Akio.; Ikeda, Sakuji.

Book ID
127191147
Publisher
American Chemical Society
Year
1970
Tongue
English
Weight
738 KB
Volume
92
Category
Article
ISSN
0002-7863

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The five-coordinate compound [RuHCl(CO)(PiPr 2 Ph) 2 ] (1), [RuHCl 2 (CO)(PiPr 2 Ph) 2 ] -contains the chloro ligands in cis and the phosphanes in trans disposition. The Ru=CH 2 bond which was prepared from RuCl 3 β€’ 3 H 2 O and PiPr 2 Ph in methanol in the presence of NEt 3 , reacts with CO and wit