Nitrogen-14 NMR and quadrupole splitting of ammonium ions in the lyotropic mesophase
β Scribed by Douglas M Chen; Jerry D Glickson
- Publisher
- Elsevier Science
- Year
- 1977
- Weight
- 446 KB
- Volume
- 28
- Category
- Article
- ISSN
- 0022-2364
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π SIMILAR VOLUMES
A new two-dimensional Fourier transform technique is proposed to unravel overlapping resonances in single crystal 14N spectra due to proton-nitrogen dipolar couplings. One frequency domain is reserved for the proton decoupled quadrupolar spectrum, while the orthogonal frequency dimension shows the d
## Abstract Analysis of the ^1^H NMR spectrum of Ξ³βhydroxypyridine dissolved in the lyotropic mesophase formed by a 14 : 1 : 1 : 20 mixture (by weight) of sodium dodecyl sulphate, decanol, sodium sulphate and D~2~O provides all the spectral parameters with reasonable precision. The chemical shift,