Nitrile Ylides—Generation of Nitrile Ylides by Thermolysis of 1,2,4-Oxazaphospholines
✍ Scribed by Klaus Burger; Annett Fuchs
- Publisher
- John Wiley and Sons
- Year
- 2004
- Weight
- 52 KB
- Volume
- 35
- Category
- Article
- ISSN
- 0931-7597
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XI SO. ( 2 0 m L ) was condensed at -190°C into a pressure flask containing l.Og (6.8 mmol) of 1 and I.0g (3.4mmol) of 3. The colorless solution was allowed to warm up in the dark to room temperature and stirred for 18 h. The moderately soluble precipitate that formed was filtered off and the soI\r