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New thiocarbonyl iridium and rhodium complexes with azolate type ligands

✍ Scribed by Josefa Reyes; Luis A. Oro; Miguel A. Ciriano; Daniel Carmona

Publisher
Springer
Year
1985
Tongue
English
Weight
227 KB
Volume
10
Category
Article
ISSN
0340-4285

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## Abstract The treatment of [M(μ‐Cl)(coe)~2~]~2~ (M = Rh, Ir; coe = cyclooctene) with the α‐diketimines ArN=C(Me)C(Me)=NAr (Ar = Ph, Xy; Xy = 2,6‐Me~2~C~6~H~3~) in thf, followed by the addition of CN__t__Bu, gave the α‐diketimine complexes [M(Cl){ArN=C(Me)C(Me)=NAr} (CN__t__Bu)] (1: M = Rh, Ar = P