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New, systematic syntheses of boron hydrides via hydride ion abstraction reactions: preparation of B2H6, B4H10, B5H11, and B10H14

✍ Scribed by Toft, Mark A.; Leach, J. B.; Himpsl, Francis L.; Shore, Sheldon G.


Book ID
120355289
Publisher
American Chemical Society
Year
1982
Tongue
English
Weight
788 KB
Volume
21
Category
Article
ISSN
0020-1669

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ChemInform Abstract: Preparation, 11B NM
✍ C. NACHTIGAL; W. PREETZ πŸ“‚ Article πŸ“… 2010 πŸ› John Wiley and Sons βš– 32 KB πŸ‘ 2 views

Preparation, 11B NMR, Vibrational Spectra, and Crystal Structure of (P( C6H5)4)2(1,10-(O2N)2B10H8). -The title compound (I) is obtained in β‰ˆ7% yield in addition to the known compounds (PPh4)3(B10H9(NO)B10H9) (β‰ˆ12%), (PPh4)(1-N2B10H9) (β‰ˆ9%); and (PPh4)2(1-(O2N)B10H9) (22%) and separated by ion excha