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New Synthetic Technologies for the Construction of Heterocycles and Tryptamines

✍ Scribed by Nicolaou, K. C.; Krasovskiy, Arkady; Majumder, Utpal; Trépanier, Vincent É.; Chen, David Y.-K.

Book ID
121356817
Publisher
American Chemical Society
Year
2009
Tongue
English
Weight
512 KB
Volume
131
Category
Article
ISSN
0002-7863

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## Experimental Section DMP (2.0 equiv) was added in one portion to a solution of 7 a (0.1 mmol) in benzene (4 mL) or BTF. [6] The solution was heated at reflux (or at 80 ± 85 8C for the reactions in BTF) for about 30 min at which point TLC indicated complete consumption of starting material. Dilu