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New synthetic route of guanidine from trichloroacetamide for tetrodotoxin and its related compounds

✍ Scribed by Toshio Nishikawa; Norio Ohyabu; Noboru Yamamoto; Minoru Isobe

Publisher: Elsevier Science
Year: 1999
Tongue: French
Weight: 991 KB
Volume: 55
Category: Article
ISSN: 0040-4020
DOI: 10.1016/s0040-4020(99)00140-4

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## Experimental Section DMP (2.0 equiv) was added in one portion to a solution of 7 a (0.1 mmol) in benzene (4 mL) or BTF. [6] The solution was heated at reflux (or at 80 ± 85 8C for the reactions in BTF) for about 30 min at which point TLC indicated complete consumption of starting material. Dilu

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## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 100 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a “Full Text” option. The original article is trackable v