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New synthetic methods in rotenoid chemistry: [7?-13C]- and [7?-14C]-(?)-rotenone and (�)-isorotenone

✍ Scribed by Carson, David; Cass, Malcolm W.; Crombie, Leslie; Holden, Ian; Whiting, Donald A.

Book ID
120263114
Publisher
Royal Society of Chemistry
Year
1982
Weight
746 KB
Volume
0
Category
Article
ISSN
1472-7781

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Determining C-7 stereochemistry in C-7-s
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✍ Samuel M. Mazza 📂 Article 📅 1993 🏛 John Wiley and Sons 🌐 English ⚖ 231 KB

## Abstract A re‐analysis of previously published ^13^C NMR data on C‐7‐substituted 6α,14α‐__endo__‐ethanotetrahydrothebaines shows that the ^13^C chemical shift of C‐18 in these medicinally important compounds can be used as an indicator of C‐7 stereochemistry, this being due to a steric gamma eff