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New synthesis of 4,5-diaryl-1,3-oxathiol-2-ones

โœ Scribed by Mikhail M. Krayushkin; Sergey N. Ivanov; Boris V. Lichitsky; Denis V. Kozhinov; Lyudmila G. Vorontsova; Zoya A. Starikova; Arkady A. Dudinov


Book ID
111730409
Publisher
Royal Society of Chemistry
Year
2004
Tongue
English
Weight
103 KB
Volume
14
Category
Article
ISSN
0959-9436

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N-Acetyl-N-methyl-3-aryl-3-[1-(aroyl)ethylthio]-2-propaneamides, prepared from thioaroylketene S,N-acetals, Hg(OAc) 2 and silyl enol ethers of aryl-1-propanones in CH 2 Cl 2 at rt, reacted with NaH in THF to give the title compounds in excellent yields.