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New siloxane-containing iron(III) carboxylate clusters

✍ Scribed by Carmen Racles; Mihaela Silion; Nicolae Stanica; Maria Cazacu; Constantin Turta

Book ID: 116680365
Publisher: Elsevier Science
Year: 2012
Tongue: English
Weight: 721 KB
Volume: 711
Category: Article
ISSN: 0022-328X
DOI: 10.1016/j.jorganchem.2012.03.024

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To a solution of (S)-1 a (290 mg, 1 mmol) in dry T H F (10 mL) at 0 'C was added dropwise nBuLi (0.7 mL of a 1.6 M solution. 1.1 mmol) under argon. The dark solution was stirred at 0 'C for 15 min and 2 h at room temperature. The mixture was cooled to 0 C and iodomethane (120 pL, 2 mniol) was inject