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New rearrangements of phosphorus-nitrogen ligands

✍ Scribed by Panova, Yu. S.; Kornev, A. N.; Sushchev, V. V.; Cherkasov, A. V.; Abakumov, G. A.

Book ID: 119881794
Publisher: Springer
Year: 2012
Tongue: English
Weight: 237 KB
Volume: 445
Category: Article
ISSN: 0012-5008
DOI: 10.1134/s0012500812080058

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## Abstract The oxidation of 1,5‐dimethyl‐2,4‐bis(diethylamino)‐1,5‐diaza‐2,4‐diphosphorinan‐6‐one __5__ with tetrachloroorthobenzoquinone (TOB) leads to the formation of the spirophosphorane __9__, which is unstable and undergoes an unusual spontaneous rearrangement into the isomeric methylenephos