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New one-pot synthesis of α-hydroxyaldehyde ethyl sulfates from terminal olefins

✍ Scribed by N. V. Zyk; E. E. Nesterov; A. N. Khlobystov; N. S. Zefirov


Book ID
112537477
Publisher
Springer
Year
1996
Tongue
English
Weight
130 KB
Volume
45
Category
Article
ISSN
1573-9171

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One-pot synthesis of γ-butyrolactones an
✍ Makoto Wada; Takahide Shigehisa; Hiroaki Kitani; Kin-ya Akiba 📂 Article 📅 1983 🏛 Elsevier Science 🌐 French ⚖ 208 KB

Lewis acid ( SnC14 ) catalyzed reaction of ethyl a-chloro-a-(p-chlorophenylthio)acetate ( l& ) with several olefins afforded the corresponding ybutyrolactones ('3) in good yields ( 51 -9wo ). Under almost the same conditions, o-(t;butylthio)-o-chloroacetone ( 2 ) reacted with olefins to give the exp