𝔖 Bobbio Scriptorium
✦   LIBER   ✦

New method of obtaining nicotinic acid from 2-methyl-5-ethylpyridine

✍ Scribed by B. V. Suvorov; V. A. Yakovlev; A. D. Kagarlitskii; É. M. Guseinov; R. T. Kutzhanov; I. I. Kan; O. B. Lebedeva

Book ID
112396550
Publisher
Springer
Year
1976
Tongue
English
Weight
276 KB
Volume
10
Category
Article
ISSN
0091-150X

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

Preparation of nicotinic-5-2H acid from
Preparation of nicotinic-5-2H acid from 5-bromonicotinic acid
✍ Brian R. Clark 📂 Article 📅 1976 🏛 John Wiley and Sons 🌐 French ⚖ 257 KB

## Abstract Methyl nicotinate‐5‐^2^H was prepared in dry tetrahydrofuran by palladium‐catalyzed deuterolysis of methyl 5‐bromonicotinate. Acid hydrolysis of the crude reaction mixture resulted in a 92% yield of deuterium‐labeled nicotinic acid of which 80 mole% was nicotinic‐5‐^2^H acid and 12 mole