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New hexanuclear antiferromagnetic heterospin iron complex

โœ Scribed by M. A. Kiskin; G. G. Aleksandrov; Yu. G. Shvedenkov; V. M. Novotortsev; I. L. Eremenko

Book ID
106520143
Publisher
Springer
Year
2006
Tongue
English
Weight
376 KB
Volume
55
Category
Article
ISSN
1573-9171

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To a solution of (S)-1 a (290 mg, 1 mmol) in dry T H F (10 mL) at 0 'C was added dropwise nBuLi (0.7 mL of a 1.6 M solution. 1.1 mmol) under argon. The dark solution was stirred at 0 'C for 15 min and 2 h at room temperature. The mixture was cooled to 0 C and iodomethane (120 pL, 2 mniol) was inject