𝔖 Bobbio Scriptorium
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New derivatives for gas chromatographic and mass spectrometric analysis of some steroid hormones

✍ Scribed by Khalid Sabih A. Razzak; Khawla A. Hamid

Publisher
John Wiley and Sons
Year
1980
Tongue
English
Weight
519 KB
Volume
7
Category
Article
ISSN
1076-5174

No coin nor oath required. For personal study only.

✦ Synopsis

Several androgenic progestins and corticosteroids were oxidized to the corresponding carbonyl-containing compounds. Oxidation was achieved by treatment with chromium trioxide under acidic conditions. The oxidation products were studied by gas chromatography and mass spectrometry. The gas chromatographic method was found to be very rapid because of the short retention times of the oxidation products. It was also found to be very sensitive for submicrogram levels. Mass spectral studies proved the structure of the products.

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