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New compounds: Synthesis of 2-amino-5H-1,3,4-benzotriazepin-5-ones

✍ Scribed by Robert W. Leiby; Ned D. Heindel


Publisher
John Wiley and Sons
Year
1977
Tongue
English
Weight
202 KB
Volume
66
Category
Article
ISSN
0022-3549

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Facile synthesis of model 1,4-dihydro-1H
✍ Bassam A. Abu Thaher; Jalal A. Zahra; Mustafa M. El-Abadelah πŸ“‚ Article πŸ“… 2002 πŸ› Journal of Heterocyclic Chemistry 🌐 English βš– 48 KB

## Abstract 2‐Aminobenzoic acid reacts readily, in the presence of triethylamine, with hydrazonoyl chlorides (**5a‐c**) (precursors of the reactive nitrile imine 1,3‐dipolar species) to afford high yields of the corresponding acyclic amidrazone adducts (**6a‐c**). The latter adducts undergo, in THF