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Natural-abundance two-dimensional solid-state silicon-29 NMR investigations of three-dimensional lattice connectivities in zeolite structures

✍ Scribed by Fyfe, Colin A.; Feng, Y.; Gies, H.; Grondey, H.; Kokotailo, G. T.

Book ID: 126261633
Publisher: American Chemical Society
Year: 1990
Tongue: English
Weight: 825 KB
Volume: 112
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja00165a002

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## Abstract In order to determine the nature and the structure of polymers formed by condensation of alkoxysilanes, a two‐dimensional INEPT double quantum filtered COSY NMR experiment was developed to observe ^29^Si^29^Si correlations at ^29^Si natural abundance. This experiment was tested on a mi