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N-nitrosamines via the phase-transfer mediated nitrosation of secondary amines with sodium nitrite and n-haloamides

✍ Scribed by Masayuki Nakajima; John C. Warner; J.-P. Anselme

Publisher: Elsevier Science
Year: 1984
Tongue: French
Weight: 211 KB
Volume: 25
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(01)81245-4

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✦ Synopsis

Secvndahy

am&m am cleanly and kieadiey convmed xo .the cotmtipandcng N-v~&~natnin~ in tigh ykLdn undti pha?le-titi1(eri concGaXati blr mQLzMn oh nodiwn nithitc and N-h&o-

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Efficient and Chemoselective N-Nitrosation of Secondary Amines under Mild and Heterogeneous Conditions with Sodium Nitrite and Oxalic Acid Dihydrate. -Under the reaction conditions the nitrogen atom is nitrosated exclusively. No nitrosation of the phenyl rings is observed in the case of (Id). In a