N-lithio-n-(2-lithioethyl)benzamide: direct preparation of a 2-lithioethylamine equivalent
✍ Scribed by José Barluenga; Francisco Foubelo; Francisco J. Fan˜anás; Miguel Yus
- Book ID
- 103401121
- Publisher
- Elsevier Science
- Year
- 1988
- Tongue
- French
- Weight
- 98 KB
- Volume
- 29
- Category
- Article
- ISSN
- 0040-4039
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 273 K Mean '(C±C) = 0.003 A Ê R factor = 0.040 wR factor = 0.112 Data-to-parameter ratio = 17.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, C 21 H 17 N 3 O 3 exhibits antifungal and antibacterial properties. The crystal structure is stabilized by a co-operative interplay of both intra-and intermolecular strong and weak hydrogen bonds of types O-HÁ Á ÁN, N-HÁ Á ÁO and C-HÁ Á ÁO/N.
## COMMUNICATIONS ence peak and hole: 310 enm-', R1 (F > 4a(F)) = 0.040 and wR2 = 0.095 (all data); R values as defined above. Data of both structures were collected on a Stoe-Siemens-AED diffractometer. The intensities of the rapidly cooled crystals in an oil drop [27] were collected by the 2 O/w