𝔖 Bobbio Scriptorium
✦   LIBER   ✦

N-Ethyl-2-(4-nitro­phen­oxy)-N-phenyl­acetamide

✍ Scribed by Ding, Yang-Jun ;Chen, Guang ;Liu, Yu-Xia

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
113 KB
Volume
62
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

The asymmetric unit of the title compound, C 16 H 16 N 2 O 4 , obtained from the reaction of 4-nitrophenol with N-ethyl-Nphenylchloracetamide in dimethylformamide at 373 K, contains two crystallographically independent molecules which differ in the orientations of the ethyl groups. The dihedral angles between the two benzene rings are 57.72 (9) and 67.78 (9) in the two molecules.

📜 SIMILAR VOLUMES

N-Benzyl-2-(4-nitro­phen­oxy)acetamide
N-Benzyl-2-(4-nitro­phen­oxy)acetamide
✍ Zhang, Yu-Liang ;Li, Xiao-Hui 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 279 KB

There are two independent molecules in the asymmetric unit of the title compound, C 15 H 14 N 2 O 4 , which differ from each other in some torsion angles. In the crystal structure, molecules are linked throgh intermolecular N-HÁ Á ÁO hydrogen bonds, forming chains running along the b axis.

2-(4-Fluoro­phen­oxy)-N-methyl­acetamide
2-(4-Fluoro­phen­oxy)-N-methyl­acetamide
✍ Luo, Zhong-Hua ;Liu, Shan ;Deng, Shui-Ping ;Zhu, Hong-Jun ;Jia, Hong-Sheng 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 274 KB

The asymmetric unit of the title compound, C~9~H~10~FNO~2~, contains two molecules. Intra- and intermolecular N—H...O and C—H...F hydrogen bonds link the molecules into a three-dimensional framework; they seem to be effective in the stabilization of the crystal structure.

2-Chloro-N-(4-nitro­phen­yl)acetamide
2-Chloro-N-(4-nitro­phen­yl)acetamide
✍ Wen, Yong-Hong ;Li, Xue-Mei ;Xu, Li-Li ;Tang, Xiao-Fang ;Zhang, Shu-Sheng 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 138 KB
4-Nitro-N-[4-(4-nitro­phen­oxy)phen­yl]b
4-Nitro-N-[4-(4-nitro­phen­oxy)phen­yl]benzamide
✍ Butt, M. Saeed ;Akhter, Zareen ;Bolte, Michael ;Siddiqi, Humaira M. ;Shamsi, Ehs 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 223 KB
2-Chloro-N-(4-chloro-2-nitro­phen­yl)ace
2-Chloro-N-(4-chloro-2-nitro­phen­yl)acetamide
✍ Zhang, Shu-Sheng ;Xu, Li-Li ;Zou, Jin ;Bi, Sai ;Wen, Yong-Hong 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 153 KB